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The solution‐based reaction in dry THF and under nitrogen atmosphere at 50 °C with either zinc flakes or granular zinc (no additive used) resulted in low yields of 7 and 4 %, respectively (Scheme 4 B), whereas under ball‐milling conditions without any solvent, inert gas, or additive (Table 2), the reaction proceeded smoothly in 2 h and all ...
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